Award

OrbiSIMS – simultaneous high-mass resolving power and high-spatial resolution mass spectrometry imaging for biological and advanced materials characterisation

  • National Physical Laboratory

F15: Voluntary ex ante transparency notice

Notice identifier: 2023/S 000-002057

Procurement identifier (OCID): ocds-h6vhtk-0399e3

Published 23 January 2023, 4:45pm



Section one: Contracting authority/entity

one.1) Name and addresses

National Physical Laboratory

Hampton Road

Teddington

TW11 0LW

Contact

Mandy Morgan

Email

mandy.morgan@npl.co.uk

Telephone

+44 2089436731

Country

United Kingdom

Region code

UK - United Kingdom

Internet address(es)

Main address

www.npl.co.uk

one.4) Type of the contracting authority

Body governed by public law

one.5) Main activity

Other activity

Research


Section two: Object

two.1) Scope of the procurement

two.1.1) Title

OrbiSIMS – simultaneous high-mass resolving power and high-spatial resolution mass spectrometry imaging for biological and advanced materials characterisation

two.1.2) Main CPV code

  • 38000000 - Laboratory, optical and precision equipments (excl. glasses)

two.1.3) Type of contract

Supplies

two.1.4) Short description

NPL pioneered the next generation OrbiSIMS technology introduced in detail in Nature Methods (2017, PMID: 29131162). The instrument is equipped with a time-of-flight mass spectrometer (ToF) for high-speed imaging of large areas or in 3D. It is also equipped with a high-field Orbitrap mass spectrometer with a mass resolving power of >240,000 at m/z 200 and a mass accuracy of approximately 1 ppm. Both ToF and Orbitrap analysers can be used simultaneously or separately. The OrbiSIMS shall be able to carry out cryogenic analysis under ultra-high vacuum with sample holder temperatures below –150 oC.

two.1.6) Information about lots

This contract is divided into lots: No

two.1.7) Total value of the procurement (excluding VAT)

Value excluding VAT: 2,254,326.75 EUR

two.2) Description

two.2.3) Place of performance

NUTS codes
  • UK - United Kingdom

two.2.4) Description of the procurement

The OrbiSIMS instrument shall be equipped with a time-of-flight mass spectrometer (ToF) for high-speed imaging of large areas or in 3D. It shall also be equipped with a high-field Orbitrap mass spectrometer with a mass resolving power of >240,000 at m/z 200 and a mass accuracy of ~ 1 ppm. The instrument shall be equipped with 3 primary ion beams which are optimal for different materials systems. (1) A 20 kV gas cluster ion source with a spatial resolution < 2 µm used for biological imaging and depth-profiling of organic materials, (2) a low energy (250 eV to 2000 eV) dual source (Cs and O2) sputter beam with high-current (>50 nA at 500 eV with a spatial resolution < 40 µm) for depth profiling of semiconductor samples and (3) a 30 kV high-resolution Bi nanoprobe with a spatial resolution < 50 nm. The instrument shall be able to operate with either the ToF analyser or the Orbitrap analyser or a combination of the two as described in the Nat. Methods paper. (4) a Ga focused ion beam with accelerating voltages of up to 30 kV, minimum bema diameter of 60nm and beam current > 25 nA. The OrbiSIMS shall be equipped for cryogenic analysis (sample holder temperature < -150 oC) and be compatible with and including Leica sample holders and allow the docking of a Leica VCT-500 cryo transfer vessel. It shall have two high-resolution TV cameras for direct sample observation and rapid location of the area of interest, as well as a photo box for high-resolution sample navigation. In addition to mass analysers, the instrument shall have a pulsed high-quality Everhart-Thornley secondary electron detector, located at grazing incidence to the sample, for primary ion induced secondary electron imaging and a self-adjusting charge compensation system using a pulsed, low energy electron flood gun. Samples shall be mounted using a rapid sample introduction system, with one sample holder for rear mounting of up to 18 samples with maximum dimensions of 10 mm x 10 mm x 8 mm, including mounting accessories, one sample holder for top mounting of multiple samples on an area of 100 mm x 80 mm with a maximum thickness of up to 20 mm, and one sample holder for mounting samples for cryogenic analysis.

two.2.11) Information about options

Options: No

two.2.13) Information about European Union Funds

The procurement is related to a project and/or programme financed by European Union funds: No


Section four. Procedure

four.1) Description

four.1.1) Type of procedure

Award of a contract without prior publication of a call for competition in the cases listed below

  • The procurement falls outside the scope of application of the regulations

Explanation:

The OrbiSIMS concept was created at NPL and the first prototype instrument was built in a collaborative project with IONTOF and ThermoFisher Scientific. The instrument was subsequently commercialised by IONTOF and sold as the Hybrid SIMS. IONTOF are the only manufacturer of this type of instrument. A number of features of the OrbiSIMS instrument are protected by international patents. Unique features of the OrbiSIMS instrument include:

1. Imaging of biomolecules from tissue using a gas cluster ion beam with a spatial resolution of < 2 µm simultaneously with a mass resolving power of > 240,000 at m/z 200.

2. Depth resolution of < 10 nm of organic molecules in an organic multilayer reference sample simultaneously with a mass resolving power of > 240,000 at m/z 200.

3. Depth resolution of < 2 nm of ions in an inorganic semiconductor delta-layer reference sample simultaneously with a mass resolving power of > 240,000 at m/z 200.

4. Cryogenic imaging (see requirement 1) with a sample holder temperature of < -150 oC. Samples shall be mounted on Leica sample mounts. The instrument shall accept docking of a Leica VCT-500 cryo transfer vessel and have provision to receive samples into the instrument.

four.1.8) Information about the Government Procurement Agreement (GPA)

The procurement is covered by the Government Procurement Agreement: No


Section five. Award of contract/concession

A contract/lot is awarded: Yes

five.2) Award of contract/concession

five.2.1) Date of conclusion of the contract

23 January 2023

five.2.2) Information about tenders

The contract has been awarded to a group of economic operators: No

five.2.3) Name and address of the contractor/concessionaire

IONTOF GmbH

Heisenbergstr 15

Munster

48149

Country

Germany

NUTS code
  • DE - Germany
The contractor/concessionaire is an SME

No

five.2.4) Information on value of contract/lot/concession (excluding VAT)

Lowest offer: 2,254,326.75 EUR / Highest offer: 2,254,326.75 EUR taken into consideration

five.2.5) Information about subcontracting

The contract/lot/concession is likely to be subcontracted


Section six. Complementary information

six.4) Procedures for review

six.4.1) Review body

NPL Management Ltd

Hampton Road

Teddington

TW11 0LW

Country

United Kingdom